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Hugo Celio and the Kratos XPS

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Information the Equipment Can Provide

This multi-technique with photoelectron and ion spectroscopies, including surface-mapping capabilities, was purchased from Kratos Analytical in 2007 to determine surface elemental and composition analysis. Most samples can be analyzed in a non-invasive or non-destructive method. This instrument is equipped with additional techniques:

  • X-ray photoelectron spectroscopy (XPS) provides information on elemental composition and chemical bonding states of materials
  • Ultraviolet photoelectron spectroscopy (UPS) provides information on valence levels and work function measurements of materials
  • Low energy Ion Scattering spectroscopy (ISS) provides provide evaluation of the elemental composition and structure of solid surfaces
  • XPS mode is also capable of surface mapping to provide lateral distribution maps of elemental and chemical species at the surface

Key Features

  • Signal detected: Photoelectron from near surface atoms
  • Elements detected: From Lithium to heavy metals
  • Detection limits: 0.1 to 1 atomic %.
  • Depth resolution: 2 to 8 nm
  • Depth Profile: 0.5 nm/second using Argon ions
  • Lateral resolution: 15 to 500 microns

The Kratos XPS is also equipped with a set of chambers and a capsule (collectively called ROX interface) to transfer air sensitive samples from an argon (or nitrogen) filled glove box to the XPS surface analysis chamber, which is under ultra-high vacuum (UHV). The Rox Interface was designed and developed at the Texas Materials Institute (U.S. Patent Application Serial No. 14/445,650 filed July 29, 2014). Unlike commercial interfaces, the Rox interface was designed with a unique innovation, as it has a built-in semi-quantitative method to monitor sample transfer reliability and validity.

Fees and Policies

  • UT Users: $60/hour
  • Higher Education/State Agencies: $212/hour
  • Corporate/External Users: $293/hour

To become a new user of this facility, please read the Instrument Reservation Information page. If you are already a user you can make a reservation in FBS.

Texas Materials Seminar Series

The Texas Materials Seminar Series features MSE 397 Seminars, TMI Distinguished Lectureships, and TMI Special Seminars, where leading faculty and professionals from around the world share cutting-edge innovations and advancements in materials engineering with our students.

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$12M+

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20+

Research Patents

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News

Subhashini Sugumar Wins in Empower Your Research Pitch Finals

Subhashini Sugumar, a Materials Science & Engineering graduate student, won the Overall Excellence in Research Communication award for her talk, "Reading a Battery's Mind."

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Yunlan Emma Zhang Awarded Outstanding Technical Contribution Award from the Aerospace Division of ASCE

Yunlan Emma Zhang, an assistant professor in the Maseeh Department of Civil, Architectural and Environmental Engineering and an affiliate faculty member of Texas Materials Institute, was recently awarded the Outstanding Technical Contribution Award from the Aerospace Division of the American Society of Civil Engineers (ASCE).

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Subhashini Sugumar Reaches Finals of University's Empower Your Research Pitch

Subhashini Sugumar, a Materials Science & Engineering graduate student in Venkat Subramanian's lab, is a finalist in the University's Empower Your Research Pitch competition with her talk "Reading a Battery's Mind."

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Gavin Latham Awarded SMART DoD Scholarship

Gavin Latham, a Materials Science & Engineering doctoral student under the supervision of Xiuling Li, has been awarded a scholarship the Science, Mathematics, and Research for Transformation (SMART) Scholarship-for-Service Program. The SMART Scholarship-for-Service Program provides scholarship recipients with full tuition, annual stipends, summer internships, and civilian employment in a DoD facility after graduation.

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Siddhartha Nanda Publishes on the Safety of K-ion Batteries

Siddhartha Nanda, a Materials Science & Engineering graduate student and member of Dr. Hadi Khani's lab, has just had an article published in Energy & Environmental Science that answers the important question, "Is a non-flammable electrolyte safer?"

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